Thermal Testing Limit Safety

Thermal Testing Limit Safety

Temperature Range Safety

Temperature chambers and hot/cold plates are invaluable tools for environmental simulation thermal testing.

Inherent in their performance capabilities are some risks, primarily the possibility of exposing items (and people) to extreme temperatures resulting in damage, injury, or combustion. When testing it is obviously important to make sure devices or samples to be tested are not exposed to temperatures outside the intended temperature range.  In cases such as flight or space hardware the cost of disqualified hardware, even if it was only briefly exposed to excessive cooling alone can be enormous.

Several approaches singularly applied or redundantly will reduce the risk of losses.

These systems are known by several names: Thermal Range safety, System Failsafe, Limit Controller, or Latching Thermostat, to name a few.  Some of these systems can be communicated with by automated test systems.

To start with, most modern temperature chambers or thermal platforms offer several levels of protection starting with the temperature controller.  Temperature controllers typically are designed to prevent users from requesting temperatures that would damage the system itself if not strictly the items under test.  Often there are locked limits that are set at the factory to protect the test equipment and additional user limits that can be set to prevent accidental damage to devices under test.  Beyond that many controllers will also go into an ALARM shutdown mode if the attached sensor reads outside the preset range.

The first way that requires thought of additional protection is for excessive or runaway heating. For example, if the output device that switches heaters sticks on, a controller alarm condition may not effectively stop runaway heating. Most systems include some sort of an additional latching thermostat that will shut down any heating when a limit temperature has been exceeded due to system problems, component failure, human error, or other causes.  The latching function keeps the heat from cycling back on if no human intervention in the form of a reset, power down, or other status confirmation has occurred.

     

Failsafe Limit controller circled                Redundant L-N2 valve assembly

Systems that are air-cooled, or cooled with single-stage refrigeration are less likely to cause damage from runaway cooling conditions but often times protection from excessively cold temperatures are required as well.  If cooling is performed using L-CO2, multiple stage refrigeration, or especially if L-N2 then cooling limit protection is also highly recommended due to the extreme temperatures possible.  Many limit protection systems can respond to both high and low limits in one unit. Protecting from extremely cold temperatures when cooling with L-N2 will often require a little additional planning.  Unlike protecting from high temperatures, removing power from the system for a cold temperature runaway event is not as likely to provide full protection from cold.  The most common example of this would be contamination causing the plunger in the L-N2 valve to stick open.  Killing the power will not likely release the plunger.  For these cases, the addition of a redundant L-N2 valve wired to the limit controller is a good choice, especially if there is a possibility of unattended or overnight testing.  The redundant valve stays energized so it is not receiving the same operational wear and tear as the control valve.

Following this thought, it is also good to look at the possibility of unintended heating due to an active load in the system or even high-velocity chamber blowers which can produce unexpectedly high temperatures. (well over 100C in the chamber is possible due to air friction alone, without the heat turned on!)  In these cases, it is good to ensure that functionality is in place to shut off possible active heat load sources in the chamber including chamber high-velocity blowers.  Keep in mind it works both ways. Blowers running after a shutdown will help cool self-heating products but also cause more heating due to air friction.

It is always a good idea to plan ahead when specifying new thermal test equipment. Existing chambers that don’t already have enough levels of built-in safety can often be retrofitted with integrated safety limit controllers that employ independent temperature sensing and internal system shut down capabilities.  If the addition of internal retrofit limit controls is not feasible, an external limit controller system can be employed to provide required levels of safety.  TotalTemp Technologies offers a variety of safety controls for hot/cold plates or chambers.

   

Selecting the Right L-N2 Coolant Delivery Hose

Selecting the Right L-N2 Coolant Delivery Hose

Expendable cryogenic liquids (L-N2 or L-CO2) deliver quick, accurate, economical, and precise cooling for testing electronic systems and components. Using the right hose will help make sure you get the best speed reliability and long-term economy out of your coolant.

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Vacuum Jacketed Delivery Hose

Liquid Nitrogen is cold!   Approximately -180°C and it delivers the precise, powerful cooling capability for thermal platforms or other thermal testing equipment.  However, due to the extremely low temperature, losses due to poorly insulated hoses can result.  When specifying an LN2 delivery hose, use a vacuum jacketed hose and the shortest comfortable length possible to minimize losses.

Liquid from the tank vaporizes immediately when it hits the warm hose and wastes time and cooling potential.

A good quality vacuum jacketed hose provides benefits in several ways

1)  Vacuum insulation, like that used for the tank is the best insulation possible to reduce losses due to the extreme temperature difference between the coolant temperature and the ambient temperature hose.

2)  Unpredictable delays are often experienced while coolant is flowing and waiting for the hose to cool down.  More predictable cooling rates of a good supply of coolant will make it easier for control algorithms to function resulting in less delay or instability of temperature.

3)  Pressure can increase several hundred times as a liquid warms and tries to vaporize in a hose that is shut off at both ends.  Quality vacuum jacketed hoses will have a built-in pressure relief valve that relieves excessive pressure that could result in unsafe pressures if a hose is shut off at both ends or from other overpressure situations.

4)  Most factories have rules about the safety hazards of water on the floor.  Less condensation on L-N2 lines is safer too. With poorly insulated non-vacuum jacketed hoses, extremely cold or long-term testing can result in frost or condensation on the L-N2 plumbing which usually ends up like water on the floor.

If usage is short-term or very intermittent, an armored, non-vacuum jacketed hose may be called for as a cost-saving measure but in most cases, the above benefits of a good quality vacuum jacketed hose are worth the extra cost.

While on the subject: a few points to know about vacuum jacketed hoses

Delays due to vaporization in the hose are worse at lower L-N2 pressures.

Be gentle, dropping or otherwise slamming a vacuum jacketed hose can result in a tiny amount or complete loss of vacuum.

If a hose shows signs of lost vacuum (sweating) –

Sweating Vacuum Jacketed hose shows loss of vacuum

it can usually be re-evacuated to make it perform properly again.

Factory tools and equipment are needed to re-evaluate and test the vacuum seal

The Pressure Relief Valve (PRV) is there for the L-N2 safety of people in the lab, don’t alter or remove it.

Pressure Relief valve with Candycane Riser

The pressure relief valve works best when the outlet is pointing generally downward.  This reduces the chances that the valve may weep, leak or stick open if it should become icy. A candy cane riser is an optional J-shaped pipe nipple that allows the proper orientation of the PRV.

When a tank will be used later, it is generally better to leave the liquid valve at the tank ON, that way the warming, vaporizing, and resulting pressure increase will return to the tank and not unnecessarily cause the Pressure Relief Valve to vent.  The PRV is there to help improve safety but it is best to not rely on it. Pressure generally will climb over 400 psi. before the valve opens. The solenoid valve on a typical hot-cold plate or chamber will in most cases not open properly at this pressure.

CONTACT US

Please reach out with any questions you have regarding LN-2 delivery hoses or hot/cold plates, temperature chambers, or other thermal test equipment!

Cryogenic Cooling Safety

Cryogenic Cooling Safety

Liquid Nitrogen (L-N2), Liquid Carbon Dioxide L- CO2) and other cryogenic coolant coolants have potential risks but can easily be safely managed like many things in the lab. The effective and rapid cooling these fluids produce is a great convenience for thermal testing.

Similar to other potential hazards such as flammable liquids, electricity, hot surfaces, chemicals, etc. Cryogenic fluids can be safely used when aware of a few basic precautions.  The main precautions are as follows:

  • The extremely cold temperatures of cryogenic liquids can cause burns.
  • Pressurized liquids and gasses require proper pressure regulation/venting.
  • Tanks are often very heavy and pose risks should they fall over.
  • In extreme cases, excessive use can displace breathable Oxygen in the air.

Taking Proper Precautions

When making or undoing connections to cryogenic fluids, always wear gloves and eye protection.  Preferably heavy leather gloves full face shield.  In General, the rule is hands-off of plumbing and devices at cryogenic temperatures.

Be aware of the controls/safety features of any cryogenic liquid delivery system. Know how to use these controls. Locate safety vents or ruptured disks that might unexpectedly produce a stream of cold vapor.  Here is a supplier’s link with more detailed LN2 safety information and an explanation of the controls on a cryogenic liquid vessel. Tanks have many built-in safety devices to prevent over-pressurization and general safety.

Never tamper with any of the safety devices on a tank and do not adapt connections other than standard LN2 designated connections. Not just your eyes and flesh but many items in the lab become damaged or behave differently at these extremely cold temperatures. For example, typical foam pipe insulation from materials such as polyethylene becomes extremely brittle and shatters at temperatures of Liquid Nitrogen which is typically -185 C.

Be aware that cryogenic liquids expand dramatically and forcefully in the process of use and also during unintended vaporization in the hose. When connecting equipment to a source of cryogenic liquid, there is often an automatic valve at the downstream connection that is normally closed.  After the system is used and the operator believes that he is safely shutting off the coolant source at the tank, an unsafe condition can be created. With a closed valve at both ends of a liquid-filled hose, the increasing pressure as the liquid warms can rupture the hose. The hand valve at the tank should only be closed when you are sure there is no cold liquid in the hose.  For this reason, our LN2 hoses employ a pressure relief valve that will limit the maximum pressure to a safe level. Likewise, any device using coolant must have a functioning exhaust to vent the spent coolant.

The contents of high pressure (~900psi) CO2 tank are stored at room temperature so although the pressure is much higher in the hose, to begin with, it does not increase as it sits in the hose.  You can close the hand valve on a CO2 tank at any time without risk.

LN2 tanks or dewars as they are known (vacuum insulated thermos-like bottles) rarely tip over due to the wider base but must be placed on a stable level footing. Slimmer High-pressure CO2 tanks are more prone to tip over and must always be restrained when stored in the lab for even short periods of time. The valve on the top of the tank can break if the tank falls over and cause very dangerous situations. LN2 tanks typically have a steel “halo” around the controls and ports at the tank. This increases the safety of many tank accidents.

CO2 and LN2 are both non-toxic and large parts of what we normally breathe.  Use of these cryogenic fluids in a normally ventilated area is not a problem however if the ventilation is abnormally low or there is a very large amount of coolant being used, an Oxygen monitoring device should be used to monitor the Oxygen level in the room. Exit the room without delay if Oxygen levels go below 20%.

CONCLUSION

Cryogenic coolants like many things in the lab are easily handled in a safe and efficient manner by paying attention in general and being aware of a few basic concerns.

TotalTemp’s Independent & Retrofitable Hi/Low Precision Failsafe System

TotalTemp’s Independent & Retrofitable Hi/Low Precision Failsafe System

Precision Failsafe System

This system provides truly independent safety and security from any failsafe issues that might occur and can be retrofitted to most existing Thermal Platforms or Temperature Chambers. This unit is intended to supply power to and protect any temperature chamber, thermal platform, or other thermal systems from selectable ranges of extreme temperatures. Designed to be easily customized to meet your unique and specific needs.

Announcing:

All our standard Thermal Platform models are now available with the CE mark. TotalTemp has recently completed the CE certification process for our standard platform models so they can be made available to the European Community. The EU countries have been asking for an alternative platform, now they have it!

Coming soon:

  • New, larger size thermal platforms.
  • Small benchtop temperature chambers.